Organic Structure Determination Using 2-D NMR Spectroscopy

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Autorentext
Jeffrey H Simpson, PhD, was Director of the Instrumentation Facility in the Department of Chemistry at M.I.T. from 2006 to 2017. Dr. Simpson's career in NMR/instrumentation research and instruction spans 20 years, and he has authored an introductory text on the subject of NMR as well as publishing a number of peer-reviewed articles. He is one of the Founding Members of the New England NMR Society and served as VP from its inception to 2017. He currently is a faculty member in the Department of Chemistry at the University of Richmond.

Klappentext

2nd edition.

Zusammenfassung
Contains 60 quality 2D NMR data sets following an introductory section describing the methodology employed. This title presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra.

Inhalt

PART I: Background and Methods1. Introduction2. Instrumental Considerations3. Data Collection, Processing, and Plotting4. 1H and 13C Chemical Shifts5. Symmetry and Topicity6. Through-Bond Effects: Spin-Spin (J) Coupling7. Through-Space Effects: the Nuclear Overhauser Effect (NOE)8. Molecular Dynamics9. Strategies for Assigning Molecules10. Strategies for Elucidating Unknown Molecular Structures

PART II: Problems11. Simple Assignment Problems12. Complex Assignment Problems13. Simple Unknown Problems14. Complex Unknown Problems15. NMR Resonance Assignment Problems16. NMR Unknown Problems